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GCMS analysis results for sample AE00007, Feb 13 2002

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Laboratory report documenting GCMS analysis of sample AE00007 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050165–000050176

Folder label: “GCMS X 1/3/02 A 1/24/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\JAN2402\7.D Vial: 6 Acq On 24 Jan 2002 5:57 pm Operator: 209 GALOS Sample GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 ' MS Integration Params: GOOFY.P Quant Time: Feb 8 11:23 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.48 152 975127 20.00 ug/1 -0.05 10) Naphthalene-d8 15.08 136 3815539 20.00 ug/1 -0.04 17) Acenaphthene-diO 20.34 164 1926171 20.00 ug/1 -0.05 29) Phenanthrene-dlO 24.76 188 2671403 20.00 ug/1 -0.05 38) Chrysene-dl2 32.78 240 1623262 20.00 ug/1 -0.05 44) Perylene-dl2 36.85 264 1120781 20.00 ug/1 -0.05

System Monitoring Compounds 37) 2,4-DDD 29.83 235 141109 4.60 ug/mL -0.24 Spiked Amount 5.000 Recovery = 92.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.15 128 1024 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.70 165 407 N.D. 25) Diethylphthalate 21.87 149 1405 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 7.D GCMS0103.M Fri Feb 08 11:23:59 2002 Page 1

NYC-WTC_000050167

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NYC-WTC_000050167Source: NYC Law Department, mirrored locally

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GCMS sample analysis report, Feb 2002 · Box DEP Box 16

NYC-WTC_000016657

Gas chromatography mass spectrometry report documenting analytical results for environmental samples processed in mid-February 2002.

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