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GCMS analysis results for sample AE00007, Feb 13 2002

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Laboratory report documenting GCMS analysis of sample AE00007 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050165–000050176

Folder label: “GCMS X 1/3/02 A 1/24/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\JAN2402\7.D Vial 6 Acq On : 24 Jan 2002 5:57 pm Operator 209 GALOS Sample : GC/MS SCAN 1/3 Inst GC/MS 209 Mise : Multiplr 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 8 11:23 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table. Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.76 178 964 N.D. 34) Anthracene 24.76 178 964 N.D. 35) Di-n-butylphthalate 26.78 149 14683 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.29 149 340 N.D. 41) Benzo(a)anthracene 32.78 228 4210 N.D. 42) Bis(2-ethylhexyl)phthalate 33.08 149 21420 N.D. 43) Chrysene 32.78 228 4210 N.D. 45) Di-n-Octylphthalate 34.83 149 1082 N.D. 46) Benzo(b)fluoranthene 35.83 2 52 101 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 36.85 252 4695 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g, h, i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 7 .D GCMS0103 .M Fri Feb 08 11:24:02 2002 Page 2

NYC-WTC_000050168

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NYC-WTC_000050168Source: NYC Law Department, mirrored locally

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GCMS sample analysis report, Feb 2002 · Box DEP Box 16

NYC-WTC_000016657

Gas chromatography mass spectrometry report documenting analytical results for environmental samples processed in mid-February 2002.

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