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GCMS analysis results sample AD29289, Jan 2002

Machine-extracted title · confidence 100%

Laboratory GCMS analysis report for sample AD29289 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036360–000036370

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File C: \HPCHEM\1\DATA\DEC1201\29289.D Vial: 24 Acq On 13 Dec 2001 1:25 am Operator: 209 GALOS Sample gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 311 rVB 411497 1099438 14.73% 2.788% 2 9.237 453 457 474 rBV 17357 86989 1.17% 0.221% 3 11.330 681 685 691 rBV 171139 387096 5.19% 0.982% 4 11.413 691 694 714 rVB 196032 524628 7.03% 1.330% 5 11.670 714 722 738 rBV2 2299001 5902735 79.11% 14.967%

6 15.277 1109 1115 1134 rBV 3174670 6981649 93.57% 17.703% 7 20.556 1683 1690 1708 rBV 3321199 7461605 100.00% 18.920% 8 24.972 2165 2171 2184 rBV2 3172517 6972460 93.44% 17.680% 9 25.119 2184 2187 2206 rVB 30498 113516 1.52% 0.288% 10 30.049 2719 2724 2732 rBV 446275 908302 12.17% 2.303%

11 33.005 3039 3046 3069 rBV2 2091670 5090669 68.22% 12.908% 12 37.099 3484 3492 3513 rBV 1365799 3908560 52.38% 9.911%

Sum of corrected areas: 39437647

29289.D GCMS1126.M Fri Dec 21 12:17:42 2001

NYC-WTC_000036365

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NYC-WTC_000036365Source: NYC Law Department, mirrored locally

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