GCMS reference standard results, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\LBD.D Vial: 3 Acq On 12 Dec 2001 1:43 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 1.49 ug/1 395788 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS#. Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1'-oxybis- 134 C6H14O3 000110-98-5 50 3 1-Propanol, 2- (2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 42 4 2 -Butanol,_ 3, 3 1/oxybis-__________ 162 C8H18O3 _______ 054305-61-2 3 9 Abundance 7 Scan 694 (11.419 min): LBD.D (-) m/z 59.05 100.00% ' 59

45 5000 103 73

—l— 11.00 11.20 11.40 11.60 11.80

KA .... 89..... j............. o - m/ z 45.00 49.59% miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 - 45 103 11.00 11.20 11.40 11.60 11.80 73 i 31 m/z 103.05 34.63% i r-r-H- 130 • i ■ ■ ■ • i • — m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087: 2-Propanol, 1,1-oxybis- 59 TTI 11.00 11.20 11.40 11.60 11.80

A 31 5000 - 45 m/ z 73.00 26.89% 103 1 ..... 1.... 72 _.............. 1 i ' ' ■ ' i ' m/z--> 30 40 50___ 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 11.00 11.20 11.40 11.60 11.80 m/ z 41.05 25.88%

m/z-> 5000 31

ii 45

75 89 103

■ ■ i ■ ■ > • । । ■ • ■ i • —I1 I ' ' ■ ' i ' ' ■ ' i ' ' ■ 1 i ■ • ■ 1 i ' 1 ' ' i ' • ' ' i 1 ' 1 ' i ' ‘ 30 40 50 60 70 80 90 100 110 120 130 T N 11.00 11.20 11.40 11.60 11.80

LBD.D GCMS1126.M Wed Dec 19 13:01:49 2001 Page 3

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