Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
NYC-WTC_000036162–000036183Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC2701\29231.D Vial: 57 Acq On : 30 Dec 2001 3:05 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 30 15:54 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.02 178 6227 N.D. 34) Anthracene 25.18 178 101 N.D. 35) Di-n-butylphthalate 27.01 149 31094 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.50 149 758 N.D. 41) Benzo(a)anthracene 33.05 228 17190 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 49300 N.D. 43) Chrysene 33.05 22 8 17190 N.D. 45) Di-n-Octylphthalate 35.03 149 3596 N.D. 46) Benzo(b)fluoranthene 36.15 252 2074 N.D. 47) Benzo(k)fluoranthene 36.16 252 786 N.D. 48) Benzo(a)pyrene 36.97 252 244 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.
(#) = qualifier out of range (m) = manual integration 29231.D GCMS1126.M Mon Dec 31 13:54:57 2001 Page 2
NYC-WTC_000036164
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