Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
NYC-WTC_000036162–000036183Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC2701\29231.D Vial: 57 Acq On : 30 Dec 2001 3:05 pm Operator: 209 GALOS Sample : GC/MS SCAN 1 ? / 18-A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 30 15:54 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update Response via DataAcq Meth
Internal Standards : : : Fri Dec 28 15:11:00 2001 Initial Calibration GCMS1126
R.T. Qlon Response N0 Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 3471656 20.00 ug/1 -0.02 10) Naphthalene-d8 15.30 136 12669803 20.00 ug/1 -0.01 17) Acenaphthene-dlO 20.57 164 6260482 20.00 ug/1 0.00 29) Phenanthrene-dlO 25.00 188 9449770 20.00 ug/1 0.00 38) Chrysene-dl2 33.05 240 6373575 20.00 ug/1 0.02 44) Perylene-dl2 37.15 264 3909953 20.00 ug/1 0.03
System Monitoring Compounds 37) 2,4-DDD 30.06 235 480044 4.62 ug/mL -0.01 Spiked Amount 5.000 Recovery = 92.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 10.69 93 219 N.D. 4) 1,3-Dichlorobenzene. 11.69 146 395 N.D. 5) 1,4-Dichlorobenzene 11.69 146 395 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 12.95 70 24316 N.D. 9) Hexachloroethane 13.33 117 232 N.D. 11) Nitrobenzene 13.36 77 131 N.D. 12) Isophorone 14.04 82 270 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 5169 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.06 162 103 N.D. 20) Dimethylphthalate 20.01 163 101 N.D. 21) 2,6-Dinitrotoluene 20.13 165 497 N.D. 22) Acenaphthylene 20.26 152 942 N.D. 23) Acenaphthene 20.55 153 194 N.D. 24) 2,4-Dinitrotoluene 21.29 165 659 N.D. 25) Diethylphthalate 22.10 149 4427 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.24 166 535 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 29231.D GCMS1126.M Mon Dec 31 13:54:53 2001 Page 1
NYC-WTC_000036163
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