NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 11 pages
GCMS method and data sheet, Dec 2001
Machine-extracted title · confidence 100%Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
NYC-WTC_000036044–000036054Folder label: “GCMS X 12/3/01 A 12/10/01”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report Data File : C:\HPCHEM\1\DATA\DEC1001\LBB.D Vial: 13 Acq On : 10 Dec 2001 10:26 pm Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 14:38 2001 Quant Results File: GCMS1126.RES Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration Abundance TIC: LBB.D 3000000
2800000
9 2600000 o’ 1 1 § 5! ! 2400000 t J 2200000
2000000
el 1800000
1600000
1400000 el
1200000
1000000
800000
600000 0 d a
400000 4 200000
0-—* r 111 PIN I I I F ==*—mF—F —1 TT Time—> i6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00 46.00
LBB.D GCMS1126.M Fri Dec 14 15:34:34 2001 Page 3
NYC-WTC_000036047
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NYC-WTC_000036047Source: NYC Law Department, mirrored locally
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NYC-WTC_000035890
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036350
Blank sample analysis report for GCMS testing showing non-detect levels for target analytes.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037219
Gas chromatography-mass spectrometry blank report for sample AD29932 analyzing nitrosamines and chlorinated compounds on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036079
Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034731
Instrument blank report confirming absence of target analytes in the analytical system prior to sample testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Filed elsewhere
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
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NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
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NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
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NYC-WTC_000036064
Laboratory commentary on GCMS scan of sample AD29135 conducted on December 18, 2001, noting recovery issues with LCS Standard.
Filed in the same folder