Laboratory data sheet recording GCMS Method 508 analysis of a blank sample for nitrosamines and chlorinated compounds.
NYC-WTC_000035664–000035673Folder label: “GCMS X 11/28/01 A 12/7/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report
Data File C: \HPCHEM\1\DATA\DEC0 6 01\LBB.D Vial: 35 Acq On 7 Dec 2001 8:52 am Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 9:40 2001 Quant Results File: GCMS1126.RES Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration_________________________ Abundance ' TIC: LBB.D
| 1.4e+07-
1.3e+07-
1.2e+07-
! i 1.16+07
1e+07
9000000
8000000
7000000
6000000 o
5000000 f 4000000 1 s S 3000000
1 2000000 1 sf II 8 1000000 o &
- — — । । — fi — . — L + — ii— — ,ir 0- ‘ I Time—> I6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00 46.00
LBB.D GCMS1126.M Wed Dec 12 11:22:10 2001 Page 3
NYC-WTC_000035667
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NYC-WTC_000035563
GCMS analysis results for sample AD28903 dated December 15, 2001, showing non-detect levels for various compounds.
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Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
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Laboratory notes indicating re-extraction is required due to low recovery and potential contamination.
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Laboratory notes identifying potential laboratory contamination by specific esters in sample AD28899.
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Lab report noting bis(2-Ethylhexyl) Sebacate detection and potential laboratory contamination in a water sample.
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Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
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Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
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Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
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Laboratory report noting detection of bis(2-Ethylhexyl)phthalate in sample AD29028 analyzed on December 18, 2001.
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Log recording sample volume, drip rates, and addition details for GCMS analysis in December 2001.
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Lab notes for sample AD29024 indicate detection of bis(2-Ethylhexyl)phthalate and no unusual compounds.
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Method blank report confirming absence of contamination during volatile organic compound testing procedures in January 2002.
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NYC-WTC_000035662
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035663
Fragmented document containing method 508 data and sample IDs processed by GCMS in late 2001.
Filed in the same folder
NYC-WTC_000035674
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
Filed in the same folder
NYC-WTC_000035678
Document containing calculated reference values for various organic compounds analyzed by GCMS.
Filed in the same folder
NYC-WTC_000035683
Laboratory notes stating the GCMS scan of sample AD28898 revealed no unusual compounds.
Filed in the same folder