NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 11 pages
GCMS method and data sheet, Dec 2001
Machine-extracted title · confidence 100%Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
NYC-WTC_000036044–000036054Folder label: “GCMS X 12/3/01 A 12/10/01”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C: \HPCHEM\ 1 \DATA\DEC10 01 \LBB. D Vial: 13 Acq On : 10 Dec 2001 10:26 pm Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 14:38 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 3 4) Anthracene 35) Di-n-butylphthalate 25.04 25.04 26.99 178 178 149 389 39187 J N.D. N.D. 0.29 ug/1 98 36) Fluoranthene 0.00 202 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 ( 0 N.D. 41) Benzo(a)anthracene 33.01 228 2573 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 1921 N.D. 43) Chrysene 33.01 228 N.D. 45) Di-n-Octylphthalate 35.02 149 133 N.D. 46) Benzo(b)fluoranthene 0.00 252 N.D. 47) Benzo(k)fluoranthene 0.00 252 N.D. 48) Benzo(a)pyrene 37.09 252 3050 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.
(#) = qualifier out of range (m) = manual integration LBB.D GCMS1126.M Fri Dec 14 15:34:28 2001 Page 2
NYC-WTC_000036046
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NYC-WTC_000036046Source: NYC Law Department, mirrored locally
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NYC-WTC_000035890
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036350
Blank sample analysis report for GCMS testing showing non-detect levels for target analytes.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037219
Gas chromatography-mass spectrometry blank report for sample AD29932 analyzing nitrosamines and chlorinated compounds on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036079
Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034731
Instrument blank report confirming absence of target analytes in the analytical system prior to sample testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Filed elsewhere
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NYC-WTC_000036041
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NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
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NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
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NYC-WTC_000036064
Laboratory commentary on GCMS scan of sample AD29135 conducted on December 18, 2001, noting recovery issues with LCS Standard.
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