Lab notes for sample AD29087 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
NYC-WTC_000035876–000035887Folder label: “GCMS X 11/30/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C: \HPCHEM\ 1\DATA\DEC13 01\29087.D Vial: 15 Acq On : 13 Dec 2001 10:48 am Operator: 209 GALOS Sample : gems scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 13 14:41 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 992094 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3809953 20.00 ug/1 -0.03 17) Acenaphthene-dl0 20.55 164 1935495 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2772762 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1700978 20.00 ug/1 -0.02 44) Perylene-dl2 37.09 264 1147384 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 187652 4.68 ug/mL -0.02 Spiked Amount 5.000 Recovery = 93.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.49 74 798 N.D. 3) bis(2-Chloroethyl)ether 11.11 93 731 N.D. 4) 1,3-Dichlorobenzene 11.59 146 422 N.D. 5) 1,4-Dichlorobenzene 11.73 146 436 N.D. 6) 1,2-Dichlorobenzene 12.23 146 313 N.D. 7) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.48 77 364 N.D. 12) 1sophorone 14.06 82 948 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.16 180 331 N.D. 15) Naphthalene 15.33 128 3245 N.D. 16) Hexachlorobutadiene 15.89 225 202 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.85 162 566 N.D. 20) Dimethylphthalate 19.96 163 1135 N.D. 21) 2,6-Dinitrotoluene 20.12 165 342 N.D. 2 2) Acenaphthylene 20.09 152 1183 N.D. 2 3) Acenaphthene 20.64 153 1411 N.D. 24) 2,4-Dinitrotoluene 21.41 165 117 N.D. 25) Diethylphthalate 22.07 149 2643 N.D. 26) 4-Chlorophenyl-phenylether 22.20 204 522 N.D. 27) Fluorene 22.18 166 1262 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 22.70 77 1735 N.D.
(#) = qualifier out of range (m) = manual integration 29087.D GCMS1126.M Thu Dec 13 14:42:48 2001 Page 1
NYC-WTC_000035878
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000037071
Laboratory commentary noting a GCMS scan of sample AD29785 revealing bis(2-Ethylhexyl)phthalate on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036603
Raw GCMS analysis data and chromatogram details for sample AD29466 including surrogate recovery results.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036995
Laboratory report of GCMS analysis for sample AD29787 conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036592
Laboratory comments on GCMS scan results for sample AD29464 noting bis(2-Ethylhexyl)phthalate at 0.48 ug/L.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036530
Laboratory commentary confirming no unusual compounds detected in sample AD29521 during GCMS scan on January 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037040
Laboratory report of GCMS analysis for sample AD29784 conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036559
Laboratory comments on GCMS scan results for sample AD29524 indicating no unusual compounds detected in the mass spectrometry analysis.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036983
Laboratory report of GCMS analysis for sample AD29786 conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036972
Laboratory report of GCMS analysis for sample AD29925 conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036581
Laboratory comments on GCMS scan results for sample AD29518 noting bis(2-Ethylhexyl)phthalate at 0.44 ug/L.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036645
Raw GCMS analysis data and chromatogram details for sample AD29517 including surrogate recovery results.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036678
Header page from a GCMS laboratory report file containing basic identification data for the analysis batch.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000035773
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035774
Laboratory data sheet recording sample volumes and drip rates for GCMS Method S08 analysis.
Filed in the same folder
NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
Filed in the same folder
NYC-WTC_000035788
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
Filed in the same folder
NYC-WTC_000035793
Document containing reference values and recovery data for organic compounds analyzed by GCMS.
Filed in the same folder