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GCMS analysis comments for sample AD29087, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29087 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.

NYC-WTC_000035876–000035887

Folder label: “GCMS X 11/30/01 A 12/10/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\DEC1301\29087.D Vial: 15 Acq On : 13 Dec 2001 10:48 am Operator: 209 GALOS Sample : gems scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant.Time: Dec 13 14:41 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 22.72 168 191 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 24.08 284 351 N.D. 3 3) Phenanthrene 25.04 178 2683 N.D. 34) Anthracene 25.18 178 1632 N.D. 35) Di-n-butylphthalate 26.99 149 35278 N.D. 36) Fluoranthene 28.68 202 1539 N.D. 39) Pyrene 29.34 202 1839 N.D. 40) Butylbenzylphthalate 31.49 149 1605 N.D. 41) Benzo(a)anthracene 33.01 228 7882 N.D. 42) Bis(2-ethylhexyl)phthalate 33.28 149 37400 0.36 ug/1 # 97 43) Chrysene 33.08 228 4025 N.D. 45) Di-n-Octylphthalate 35.03 149 3697 N.D. 46) Benzo(b)fluoranthene 36.10 252 4816 N.D. 47) Benzo(k)fluoranthene 36.12 252 2852 N.D. 48) Benzo(a)pyrene 36.94 252 1163 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29087.D GCMS1126.M Thu Dec 13 14:42:52 2001 Page 2

NYC-WTC_000035879

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NYC-WTC_000035879Source: NYC Law Department, mirrored locally

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