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GCMS analysis comments for sample AD29139, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.

NYC-WTC_000035853–000035864

Folder label: “GCMS X 11/30/01 A 12/10/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data Pile : C:\HPCHEM\1\DATA\DEC1001\29139.D Vial: 11 Acq On : 10 Dec 2001 8:30 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.602 275 279 291 rBV 357946 922766 13.67% 2.684% 2 7.740 291 294 312 rVB 35480 143721 2.13% 0.418% 3 11.348 683 687 692 rBV 53849 122883 1.82% 0.357% 4 11.430 692 696 705 rVB 57722 151076 2.24% 0.439% 5 11.669 716 722 740 rBV 2011337 4863166 72.07% 14.144% 6 15.277 1109 1115 1133 rBV 2862210 6228143 92.29% 18.113% 7 20.546 1683 1689 1713 rBV 2963659 6748113 100.00% 19.626% 8 24.971 2164 2171 2183 rBV2 2905188 6214519 92.09% 18.074% 9 26.982 2386 2390 2407 rBV 32840 73033 1.08% 0.212% 10 30.048 2718 2724 2731 rBV 425062 860568 12.75% 2.503% 11 33.004 3039 3046 3059 rBV2 1926625 4470568 66.25% 13.002% 12 37.099 3484 3492 3512 rBV2 1245417 3585473 53.13% 10.428%

Sum of corrected areas: 34384029

29139.D GCMS1126.M Wed Dec 12 16:06:46 2001

NYC-WTC_000035858

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NYC-WTC_000035858Source: NYC Law Department, mirrored locally

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