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GCMS blank results for sample AD29022, Dec 17 2001

Machine-extracted title · confidence 95%

Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.

NYC-WTC_000035776–000035787

Folder label: “GCMS X 11/30/01 A 12/10/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\LB.D Vial: 3 Acq On : 10 Dec 2001 11:42 am Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 7.59 3.83 ug/1 907560 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2- (3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 278 (7.594 mln' : LB.D (-) m/z 73.00100.00% 73 1

5000 43 1-p-n-r-j-r-n-lH- TTIIXTruur 103 7.20 7.40 7.60 7.80 8.00 37, |, I 49 55.. 67, i , 87 -n-p-r-n-p PITTTH TTpTEBDOgT l ■ • i • i n p •. . । , i । , . . . p > m/z 43.0.5 26.32% mlz- 10 20 30 40 50 60 70 80 90 100 11. 120 Abundance' #62932: Silane, tetramethyl- 73

5000 T-T-r-r-r-r-rr-r 7.20

15 45 I 53 59 88 m/z 7.40 L 10.08% 7.60 7.80 8.00

T1BB—B—————igrtmevrupr 1 | I TT I TT I I • | f I : I | I I I I | ! T miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73 1111 TInmPTIT 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.05 9.10% 44 58 15 TIT r-p-m-jH + I TT — 1 1 ■ ■ ■ i ‘ ‘ • i ■ ■ ‘ 1 i ‘ ‘ ' i ■ ■ • ‘ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet TTTmar — — H TTmrur 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0.0 6.56% 5000 45 36 55 67. TTPTTr । | 4-r __ ________ 109115 Tj 1TTT1T48 ’11nn.tIT161I~T TI TT I I II T TI TTIm TTT TT T T m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

LB.D GCMS1126.M Thu Dec 13 10:55:06 2001 Page 1

NYC-WTC_000035782

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NYC-WTC_000035782Source: NYC Law Department, mirrored locally

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