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GCMS comments for sample AD28860, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD28860 indicate no unusual compounds detected but recovery was below acceptance range.

NYC-WTC_000035765–000035772

Folder label: “GCMS X 11/28/01 A 12/7/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC0701\28860.D Vial: 6 Acq On 7 Dec 2001 7:49 pm Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 11 15:46 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.97 178 1251 N.D. 34) Anthracene 24.97 178 1251 N.D. 35) Di-n-butylphthalate 26.98 149 25921 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 4937 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 4485 N.D. 43) Chrysene 33.02 228 4937 N.D. 45) Di-n-Octylphthalate 35.03 149 185 N.D. 46) Benzo(b)fluoranthene 36.06 252 303 N.D. 47) Benzo(k)fluoranthene 36.06 252 603 N.D. 4 8) Benzo(a)pyrene 37.10 252 5085 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28860.D GCMS1126.M Wed Dec 12 10:56:05 2001 Page 2

NYC-WTC_000035768

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NYC-WTC_000035768Source: NYC Law Department, mirrored locally

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