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GCMS analysis comments, sample AD28964, Dec 2001

Machine-extracted title · confidence 90%

Lab report noting bis(2-Ethylhexyl)phthalate detection, recovery issues, and low pH.

NYC-WTC_000035640–000035650

Folder label: “GCMS X 11/29/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\DEC0701\28964.D Vial: 10 Acq On 7 Dec 2001 11:43 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 14:48 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.03 178 152 N.D. 34) Anthracene 25.03 178 152 N.D. 35) Di-n-butylphthalate 26.99 149 26335 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.50 149 986 N.D. 41) Benzo(a)anthracene 33.01 228 3746 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 39418 0.43 ug/1 96 43) Chrysene 33.01 228 3746 N.D. 45) Di-n-Octylphthalate 35.02 149 638 N.D. 46) Benzo(b)fluoranthene 36.06 252 174 N.D. 47) Benzo(k)fluoranthene 36.06 252 174 N.D. 48) Benzo(a)pyrene 37.10 252 4208 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo (g,h, i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28964.D GCMS1126.M Thu Dec 13 14:56:35 2001 Page 2

NYC-WTC_000035643

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NYC-WTC_000035643Source: NYC Law Department, mirrored locally

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