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Document / 11 pages

GCMS analysis comments, sample AD28970, Dec 2001

Machine-extracted title · confidence 90%

Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.

NYC-WTC_000035651–000035661

Folder label: “GCMS X 11/29/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\DEC0 701\28970.D Vial: 15 Acq On 8 Dec 2001 4:35 am Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 14:51 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.05 178 243 N.D. 34) Anthracene 25.05 178 243 N.D. 35) Di-n-butylphthalate 26.99 149 26755 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.50 149 1426 N.D. 41) Benzo(a)anthracene 33.01 228 4006 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 52044 0.49 ug/1 93 43) Chrysene 33.01 228 4006 N.D. 45) Di-n-Octylphthalate 35.13 149 273 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.10 252 4514 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28970.D GCMS1126.M Thu Dec 13 15:38:30 2001 Page 2

NYC-WTC_000035654

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NYC-WTC_000035654Source: NYC Law Department, mirrored locally

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