GCMS sample preparation log, Dec 2001

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LSC Area Percent Report

* Data File C:\HPCHEM\l\DATA\DEC0601\LBA.D Vial: 24 Acq On 6 Dec 2001 10:07 pm Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.671 717 722 749 rBV 1895429 5063894 71.46% 14.130% 2 15.279 1109 1115 1133 rBV 3078514 6636871 93.65% 18.520% 3 20.558 1683 1690 1714 rBV 3060053 7086742 100.00% 19.775% 4 24.974 2164 2171 2183 rBV2 3016430 6604507 93.20% 18.429% 5 25.111 2183 2186 2196 rVB 22978 71683 1.01% 0.200%

6 28.802 2583 2588 2601 rBV 89825 203606 2.87% 0.568% 7 30.050 2719 2724 2734 rBV 422050 836479 11.80% 2.334% 8 32.153 2948 2953 2957 rBV 53345 103425 1.46% 0.289% 9 33.006 3039 3046 3066 rBV2 2042122 .4883415 68.91% 13.627% 10 33.291 3072 3077 3085 rBV2 35437 86008 1.21% 0.240%

11 37.101 3484 3492 3514 rBV2 1525620 4260124 60.11% 11.888%

Sum of corrected areas: 35836754

LBA.D GCMS1126.M Wed Dec 12 11:39:04 2001

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