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GCMS blank analysis results, Jan 2002

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Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.

NYC-WTC_000019049–000019060

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data' File : C:\HPCHEM\1\DATA\DEC2701\LBA.D Vial: 4 Acq On : 27 Dec 2001 1:06 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling . : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.611 276 280 294 rBV 461756 1273971 16.77% 3.239% 2 7.758 294 296 308 rVB 38282 146717 1.93% 0.373% 3 11.678 718 723 749 rBV 2175793 5609901 73.84% 14.262% 4 14.313 1004 1010 1017 rVB 101351 213370 2.81% 0.542% 5 15.286 1110 1116 1135 rBV 2832560 6994558 92.07% 17.782%

6 17.452 1347 1352 1359 rBV 136641 279064 3.67% 0.709% 7 20.280 1654 1660 1666 rBV2 84643 167974 2.21% 0.427% 8 20.565 1685 1691 1713 rBV 3241908 7597190 100.00% 19.314% 9 21.097 1744 1749 1762 rBV2 19961 97627 1.29% 0.248% 10 22.795 1928 1934 1939 rBV 45280 93534 1.23% 0.238%'

11 24.990 2166 2173 2209 rBV2 2587601 7130722 93.86% 18.128% 12 27.018 2389 2394 2406 rBV 31584 100062 1.32% 0.254% 13 30.066 2720 2726 2740 rBV 443995 995041 13.10% 2.530% 14 33.022 3042 3048 3074 rBV2 1829209 4923908 64.81% 12.518% 15 37.117 3486 3494 3519 rBV2 1090126 3712308 48.86% 9.437%

Sum of corrected areas: 39335947

LBA.D GCMS1126.M Fri Dec 28 15:07:07 2001

NYC-WTC_000019053

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NYC-WTC_000019053Source: NYC Law Department, mirrored locally

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