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GCMS blank control analysis, organic compounds, February 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry blank control results for sample AE01937, confirming all tested organic compounds are below minimum detection limits.

NYC-WTC_000003832–000003838

Folder label: “GCMS X 1/28/02 A 2/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\LBA.D Vial: 15 Acq On 8 Feb 2002 10:57 pm Operator: 209 GALOS Sample GC/MS SCAN 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.346 790 795 811 rVB 797534 1839753 74.52% 15.002% 2 15.990 1186 1192 1207 rBV 1146821 2288284 92.68% 18.659% 3 21.306 1765 1771 1787 rBV 1273113 2468908 100.00% 20.132% 4 25.758 2249 2256 2267 rBV 1112303 2368261 95.92% 19.312% 5 27.714 2465 2469 2476 rBV 26060 48016 1.94% 0.392%

6 30.835 2803 2809 2814 rBV 125237 233355 9.45% 1.903% 7 33.828 3128 3135 3150 rBV 799129 1739070 70.44% 14.181% 8 38.115 3594 3602 3617 rBV2 430923 1277742 51.75% 10.419%

Sum of corrected areas: 12263389

LBA.D GCMS0208.M Thu Feb 14 15:03:46 2002

NYC-WTC_000003836

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NYC-WTC_000003836Source: NYC Law Department, mirrored locally

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