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GCMS blank analysis results, Feb 2002

Machine-extracted title · confidence 95%

Blank sample analysis report for GCMS testing showing non-detectable levels of target compounds on February 21, 2002.

NYC-WTC_000009710–000009715

Folder label: “GCMS X 1/17/02 A 2/17/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

- Data File : C:\HPCHEM\l\DATA\FEB1502\LBC.D Vial: 31 Acq On : 16 Feb 2002 10:28 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.208 342 345 356 rBV 11680 28718 1.14% 0.235% 2 12.330 789 794 807 rVB 857381 1919045 76.46% 15.728% 3 15.974 1185 1191 1203 rBV 1184359 2325664 92.67% 19.060% 4 21.290 1763 1770 1785 rBV 1275611 2509748 100.00% 20.569% 5 25.733 2248 2254 2266 rBV2 1089977 2335679 93.06% 19.143%

6 30.810 2802 2807 2813 rBV 120841 222905 8.88% 1.827% 7 33.802 3126 3133 3153 rBV2 741538 1632946 65.06% 13.383% 8 38.090 3591 3600 3619 rBV 413909 1226812 48.88% 10.055%

Sum of corrected areas: 12201517

LBC.D GCMS0208.M Thu Feb 21 09:30:59 2002

NYC-WTC_000009712

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NYC-WTC_000009712Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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