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GCMS blank analysis for sample AE00005, Feb 8 2002

Machine-extracted title · confidence 100%

Blank analysis report for GCMS testing of sample AE00005 showing non-detectable levels of target compounds.

NYC-WTC_000050079–000050087

Folder label: “GCMS X 1/3/02 A 1/24/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN2402\LB.D Vial: 3 Acq On : 24 Jan 2002 2:01 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.429 256 260 280 rBV 344425 971072 14.87% 2.865% 2 11.487 697 702 723 rBV 2003833 4989352 76.42% 14.718% 3 14.130 985 990 995 rBV 153814 295096 4.52% 0.871% 4 15.076 1088 1093 1108 rBV 3067437 6328005 96.92% 18.667% 5 20.346 1660 1667 1687 rBV 3107092 6528996 100.00% 19.260%

6 24.752 2141 2147 2160 rBV2 2839468 6207787 95.08% 18.313% 7 29.829 2695 2700 2710 rBV 415660 854252 13.08% 2.520% 8 32.785 3015 3022 3046 rBV 1870899 4333620 66.37% 12.784% 9 36.843 3457 3464 3488 rBV2 1230629 3390988 51.94% 10.003%

Sum of corrected areas: 33899168

LB.D GCMS0208.M Fri Feb 08 13:45:34 2002

NYC-WTC_000050083

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NYC-WTC_000050083Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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