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GCMS analysis report, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS results for sample AD28171 analyzed on January 2, 2002.

NYC-WTC_000035365–000035380

Folder label: “GCMS X 11/26/01 A 12/22/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\l\DATA\DEC2101\28172.D Vial: 38 ■Acq On : 22 Dec 2001 2:53 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Smoothing OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs 0.2 Max Peaks: 100 Stop Thrs 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.143 30 33 43 rVB 44093 83684 1.32% 0.247% 2 6.399 166 170 176 rBV 60464 108798 1.72% 0.322% 3 6.500 176 181 185 rBV 111229 207796 3.28% 0.614% 4 6.628 192 195 203 rVB 41589 82800 1.31% 0.245% 5 6.747 203 208 216 rBV 66561 138623 2.19% 0.410%

6 7.765 315 319 330 rBV 454427 923792 14.59% 2.731% 7 10.223 583 587 594 rBB 103668 180549 2.85% 0.534% 8 10.434 605 610 619 rBB 123515 213085 3.36% 0.630% 9 10.755 641 645 652 rBV 103391 190673 3.01% 0.564% 10 11.782 752 757 767 rBV 2314467 4865643 76.84% 14.385%'

11 15.395 1144 1151 1168 rBV 2852177 6332531 100.00% 18.722% 12 20.668 1719 1726 1739 rBV 2706354 6146913 97.07% 18.173% 13 25.078 2200 2207 2218 rBV2 2714030 5905580 93.26% 17.460% 14 33.084 3073 3080 3093 rBV2 2081170 4830183 76.28% 14.281% 15 37.155 3516 3524 3541 rBV2 1362548 3612957 57.05% 10.682%

Sum of corrected areas: 33823607

28172.D NP112701.M Fri Dec 28 09:08:07 2001

NYC-WTC_000035371

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NYC-WTC_000035371Source: NYC Law Department, mirrored locally

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