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GCMS reference data for sample AD28750, Dec 2001

Machine-extracted title · confidence 100%

Reference sheet listing expected values and detection limits for volatile organic compounds in WTC samples.

NYC-WTC_000035244–000035248

Folder label: “GCMS X 11/26/01 A 12/6/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC0 501\REF.D Vial: 12 Acq On 5 Dec 2001 11:21 pm Operator: 209 GALOS Sample 11/26 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 15:40 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.62 168 ' 122702 3.07 ug/1 94 31) 4-Bromophenyl-phenylether 23.68 248 79016 3.57 ug/1 95 3 2) Hexachl orobenzene 24.11 284 85519 3.51 ug/1 99 3 3) Phenanthrene 25.07 178 432168 3.63 ug/1 98 34) Anthracene 25.21 178 389787 3.28 ug/1 100 . 35) Di-n-butylphthalate 27.01 149 597995 3.77 ug/1 99 36) Fluoranthene 28.68 202 395726 3.44 ug/1 98 3 9) Pyrene 29.35 202 409994 3.37 ug/1 100 40) Butylbenzylphthalate 31.51 149 153056 2.41 ug/1 90 41) Benzo(a)anthracene 32.98 228 275925 3.29 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.31 149 212347 2.47 ug/1 100 43) Chrysene 33.11 228 308650 3.75 ug/1 99 45) Di-n-Octylphthalate 35.06 149 186977 1.52 ug/1 # 95 46) Benzo(b)fluoranthene 36.06 252 210304 3.01 ug/1 98 47) Benzo(k)fluoranthene 36.12 252 246381 3.44 ug/1 99 48) Benzo(a)pyrene 36.95 252 162972 2.68 ug/1 99 49) Indeno(1,2,3-cd)pyrene 40.81 276 175325 2.89 ug/1 99 5 0) Dibenz(a,h)anthracene 40.88 278 155099 3.26 ug/1 98 51) Benzo(g,h,i)perylene 41.91 276 158808 3.06 ug/1 95

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Fri Dec 07 15:41:40 2001 Page 2

NYC-WTC_000035247

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NYC-WTC_000035247Source: NYC Law Department, mirrored locally

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