GCMS analysis comments for sample AD28664, Dec 2001

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Quantitation Report (QT 2- d) Data File C:\HPCHEM\1\DATA\DEC0401\28664.D '‘■ "1 3 Acq On 5 Dec 2001 4:58 am C: or 09 GALOS Sample gc/ms 11/24 C/MS 209 Mise : U .00 MS Integration Params: RTEINT.P Quant Time: Dec 5 5:46 2001 Quant Re Su It" T ' 2. c : .CMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTF I Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Qvalue 33) Acenaphthylene 0.00 152 3 34) Acenaphthene 0.00 153 0 35) 2,4-Dinitrophenol 0.00 184 0 36) 4-Nitrophenol 0.00 65 ■3 37) 2,4-Dinitrotoluene 21.43 165 110 38) Diethylphthalate 22.11 149 353 39) 4-Chlorophenyl-phenylether 0.00 204 0 40) Fluorene 0.00 166 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 44) N-Nitrosodiphenylamine 0.00 168 c 45) 4-Bromophenyl-phenylether 0.00 248 46) Hexachlorobenzene 0.00 284 3 47) Pentachlorophenol 0.00 266 ) 48) Phenanthrene 25.00 178 102 2 49) Anthracene 25.00 178 1022 50) Di-n-butylphthalate 27.01 149 313 2 s 51) Fluoranthene 0.00 202 54) Pyrene 0.00 202 55) Butylbenzylphthalate 31.57 149 796 56) Benzo(a)anthracene 33.04 228 360 57) Bis(2-ethylhexyl)phthalate 33.32 149 856 0 58) Chrysene 33.04 228 360- 60) Di-n-Octylphthalate 0.00 149 61) Benzo(b)fluoranthene 0.00 252 ) 62) Benzo(k)fluoranthene 0.00 252 0 63) Benzo(a)pyrene 37.14 252 4165 64) Indeno (1,2, 3-cd) pyrene 0.00 276 । 65) Dibenz (a, h) anthracene 0.00 278 66) Benzo(g,h,i)perylene 0.00 276

(#) = qualifier out of range (m) = manual integration 28664. D GCMS1126.M Thu Dec 06 14:51:23 2001 Page 2

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