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GCMS analysis comments for sample AD28694, Dec 2001

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Laboratory report noting di-n-butylphthalate detection and low pH with recovery data for sample AD28694.

NYC-WTC_000035135–000035152

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\DEC0401\28694.D Vial: 5 Acq On : 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 4 17:05 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.16 65 325 N.D. 37) 2,4-Dinitrotoluene 20.99 165 302 N.D. 38) Diethylphthalate 22.10 149 1210 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.02 178 885 N.D. 49) Anthracene 25.02 178 885 N.D. 50) Di-n-butylphthalate 27.01 149 50394 0.29 ug/1 97 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.52 149 478 N.D. 56) Benzo(a)anthracene 33.04 228 3896 N.D. 57) Bis(2-ethylhexyl)phthalate 33.32 149 15124 N.D. 58) Chrysene 33.04 228 3896 N.D. 60) Di-n-Octylphthalate 35.08 149 176 N.D. 61) Benzo(b)fluoranthene 36.09 252 318 N.D. 62) Benzo(k)fluoranthene 36.14 252 341 N.D. 63) Benzo(a)pyrene 37.14 252 4799 N.D. 64) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28694.D GCMS1126.M Thu Dec 06 12:49:52 2001 Page 2

NYC-WTC_000035137

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NYC-WTC_000035137Source: NYC Law Department, mirrored locally

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