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GCMS analysis comments for sample AD28693, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting TurboVap contamination with recovery data for sample AD28693.

NYC-WTC_000035089–000035105

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC0401\28693.D Vial: 8 Acq On : 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 4 20:01 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

3 3) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.16 65 111 N.D. 37) 2,4-Dinitrotoluene 21.15 165 175 N.D. 38) Diethylphthalate 22.10 149 928 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 4 7) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.01 178 788 N.D. 49) Anthracene 25.01 178 788 N.D. 50) Di-n-butylphthalate 27.01 149 24943 N.D. 51) Fluoranthene 0.00 202 0 N.D. ' 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.57 149 618 N.D. 56) Benzo(a)anthracene 33.04 228 3082 N.D. 57) Bis(2-ethylhexyl)phthalate 33.32 149 4387 N.D. 58) Chrysene 33.04 228 3082 N.D. 60) Di-n-Octylphthalate 35.05 149 179 N.D. 61) Benzo(b)fluoranthene 0.00 252 0 N.D. 62) Benzo(k)fluoranthene 0.00 252 0 N.D. 6 3) Benzo(a)pyrene 37.13 252 3048 N.D. 64) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo (g, h, i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28693.D GCMS1126.M Thu Dec 06 12:47:10 2001 Page 2

NYC-WTC_000035091

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NYC-WTC_000035091Source: NYC Law Department, mirrored locally

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