GCMS analysis comments for sample AD28695, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT R viewed) Data File C:\HPCHEM\l\DATA\DEC0401\28695.D Vial: 10 Acq On 4 Dec 2001 9:10 pm C p e ra - or : 2 09 GALOS Sample gc/ms 11/24 Inst : IC/MS 209 Mise Ml- 1r: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 4 21:58 2001 Quant Result3 Pile: ICMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response C- n. Qvalue

33) Acenaphthylene 0.00 152 0 34) Acenaphthene 0.00 153 0 35) 2,4-Dinitrophenol 0.00 184 0 36) 4-Nitrophenol 0.00 65 0 37) 2,4-Dinitrotoluene 21.01 165 192 2 38) Diethylphthalate 22.12 149 109 1] D 39) 4-Chlorophenyl-phenylether 0.00 204 0 40) Fluorene 0.00 166 0 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 -T

43) 4,6-Dinitro-2-methylphenol 0.00 198 0 44) N-Nitrosodiphenylamine 0.00 168 0 45) 4-Bromophenyl-phenylether 0.00 248 0 46) Hexachlorobenzene 0.00 284 0 47) Pentachlorophenol 0.00 266 0 48) Phenanthrene 25.00 178 828 49) Anthracene 25.00 178 828 50) Di-n-butylphthalate 27.02 149 8 654 51) Fluoranthene 0.00 202 0 54) Pyrene 0.00 202 0 55) Butylbenzylphthalate 0.00 149 0 56) Benzo(a)anthracene 33.04 228 274 5 57) Bis(2-ethylhexyl)phthalate 33.31 149 2 93 9 58) Chrysene 33.04 228 2745 60) Di-n-Octylphthalate 0.00 149 61) Benzo(b)fluoranthene 0.00 252 62) Benzo(k)fluoranthene 0.00 252 G 63) Benzo(a)pyrene 37.13 252 3080 64) Indenod, 2,3-cd) pyrene 0.00 276 0 J 65) Dibenz (a, h) anthracene 0.00 278 0 66) Benzo(g,h,i)perylene 0.00 276 0

(#) = qualifier out of range (m) = manual integration 28695.D GCMS1126.M Thu Dec 06 14:47:06 2001 Page 2

NYC-WTC_000035108