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GCMS analysis comments for sample AD28690, Dec 2001

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Laboratory report noting bis(2-ethylhexyl)phthalate detection and recovery data for sample AD28690.

NYC-WTC_000035044–000035051

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\DEC0401\28690.D Vial: 20 Acq On : 5 Dec 2001 6:55 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 5 7:43 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.18 65 180 N.D. 37) 2,4-Dinitrotoluene 21.25 165 102 N.D. 38) Diethylphthalate 22.10 149 759 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.00 178 906 N.D. 49) Anthracene 25.00 178 906 N.D. 50) Di-n-butylphthalate 27.02 149 32940 N.D. 51) Fluoranthene 0.00 202 0 N.D. s 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.52 149 671 N.D. 56) Benzo(a)anthracene 33.04 228 2745 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 28294 0.40 ug/1 99 58) Chrysene 33.04 228 2745 N.D. 60) Di-n-Octylphthalate 0.00 149 0 N.D. 61) Benzo(b)fluor anthene 0.00 252 0 N.D. 62) Benzo(k)fluoranthene 0.00 252 0 N.D. 63) Benzo(a)pyrene 37.13 252 2667 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28690.D GCMS1126.M Thu Dec 06 12:40:48 2001 Page 2

NYC-WTC_000035046

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NYC-WTC_000035046Source: NYC Law Department, mirrored locally

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