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GCMS analysis results for sample AD28470, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD28470 conducted on November 30, 2001.

NYC-WTC_000034393–000034401

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2 701\28470.D Vial: 20 Acq On : 28 Nov 2001 1:48 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 29 12:40 2001 Quant Results File: GCMS1126.RES Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 20.11 152 3398 N.D. 34) Acenaphthene 20.66 153 4032 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.16 65 281 N.D. 37) 2,4-Dinitrotoluene 21.29 165 124 N.D. 38) Diethylphthalate 22.09 149 4426 N.D. 39) 4-Chlorophenyl-phenylether 22.23 204 1366 N.D. 40) Fluorene 22.20 166 3399 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 22.69 77 3121 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 22.63 168 978 N.D. 45) 4-Bromophenyl-phenylether 23.68 248 588 N.D. 46) Hexachlorobenzene 24.10 284 8 94 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.06 178 6216 N.D. 49) Anthracene 25.06 178 6216 N.D. 50) Di-n-butylphthalate 27.00 149 39824 N.D. 51) Fluoranthene 28.68 202 " 3677 N.D. 54) Pyrene 29.35 202 4215 N.D. 55) Butylbenzylphthalate 31.51 149 1746 N.D. 56) Benzo(a)anthracene 33.10 228 9423 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 3509 N.D. 58) Chrysene 32.97 228 8754 N.D. 60) Di-n-Octylphthalate 35.04 149 2588 N.D. 61) Benzo(b)fluoranthene 36.07 252 2882 N.D. 62) Benzo(k)fluoranthene 36.12 252 4675 N.D. 63) Benzo(a)pyrene 36.95 252 2067 N.D. 64) Indenod, 2,3-cd) pyrene 40.83 276 1261 N.D. 65) Dibenz(a,h)anthracene 40.91 278 696 N.D. 66) Benzo(g,h,i)perylene 41.93 276 1405 N.D.

(#) = qualifier out of range (m) = manual integration 28470.D GCMS1126.M Thu Nov 29 12:41:30 2001 Page 2

NYC-WTC_000034396

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NYC-WTC_000034396Source: NYC Law Department, mirrored locally

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