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GCMS comments for sample AD28157, Nov 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

NYC-WTC_000033800–000033815

Folder label: “GCMS X 11/20/01 A 11/26/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\NOV2 601\28157.D Vial: 16 Acq On : 27 Nov 2001 1:22 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 28 8:26 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 33) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.01 165 198 N.D. 38) Diethylphthalate 22.09 149 807 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.07 178 194 N.D. 49) Anthracene 25.07 178 194 N.D. 50) Di-n-butylphthalate 27.00 149 4289 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 0.00 149 0 N.D. 5 6) Benzo(a)anthracene 33.03 228 2783 N.D. 57) Bis(2-ethylhexyl)phthalate 33.30 149 9265 N.D. 58) Chrysene 33.10 228 1190 N.D. 60) Di-n-Octylphthalate 35.05 149 5992 N.D. 61) Benzo(b)fluoranthene 36.06 252 3887 N.D. 62) Benzo(k)fluoranthene 36.13 252 4484 N.D. 63) Benzo(a)pyrene 36.95 252 3113 N.D. 64) Indenod, 2,3-cd)pyrene 40.84 276 2291 N.D. 65) Dibenz(a,h)anthracene 40.88 278 1557 N.D. 66) Benzo(g,h,i)perylene • 41.89 276 2720 N.D.

(#) = qualifier out of range (m) = manual integration 28157.D GCMS1126.M Wed Nov 28 08:30:08 2001 Page 2

NYC-WTC_000033803

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NYC-WTC_000033803Source: NYC Law Department, mirrored locally

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Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.

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