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GCMS analysis results for sample AD28470, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD28470 conducted on November 30, 2001.

NYC-WTC_000034393–000034401

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2701\28470.D Vial: 20 Acq On : 28 NOV 2001 1:48 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 29 12:40 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.69 152 1063557 20.00 ug/1 0.00 15) Naphthalene-d8 15.30 136 4024297 20.00 ug/1 0.00 2 6) Acenaphthene-dl0 20.57 164 1888013 20.00 ug/1 0.00 42) Phenanthrene-diO 25.00 188 2457816 20.00 ug/1 0.00 53) Chrysene-dl2 33.02 240 1032280 20.00 ug/1 -0.01 59) Perylene-dl2 37.11 264 643642 20.00 ug/1 0.00 System Monitoring Compounds 52) 2,4-DDD 30.07 235 94535 3.23 ug/mL 0.00 Spiked Amount 5.000 Recovery = 64.60% Target Compounds Qvalue 2) Pyridine 5.53 79 9704 N.D. 3) N-nitroso-dimethyl amine 5.47 74 1459 N.D. 4) Phenol 11.04 94 2705 N.D. 5) bis(2-Chloroethyl)ether 11.14 93 2203 N.D. 6) 2-Chlorophenol 11.29 128 714 N.D. 7) 1,3-Dichlorobenzene 11.59 146 964 N.D. 8) 1,4-Dichlorobenzene 11.74 146 1157 N.D. 9) 1,2-Dichlorobenzene 12.26 146 850 N.D. 10) 2-Methylphenol 12.65 108 1029 N.D. 11) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 12) 3&4-Methylphenol 13.07 108 454 N.D. 13) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 14) Hexachloroethane 0.00 117 0 N.D. 16) Nitrobenzene 13.41 77 1202 N.D. 17) Isophorone 14.05 82 2863 N.D. 18) 2- Nitrophenol 14.35 139 261 N.D. 19) 2,4-Dimethylphenol 14.48 107 418 N.D. 20) bis(2-Chloroethoxy)methane 14.72 93 906 N.D. 21) 2,4-Dichlorophenol 0.00 162 0 N.D. 22) 1,2,4-Trichlorobenzene 15.19 180 1223 N.D. 2 3) Naphthalene 15.36 128 5629 N.D. 24) Hexachlorobutadiene 15.91 225 534 N.D. 25) 4-Chloro-3-methylphenol 17.21 107 729 N.D. 2 7) Hexachlorocyclopentadiene 0.00 237 0 N.D. 28) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 18.86 162 2868 N.D. 31) Dimethylphthalate 19.96 163 3840 N.D. 32) 2,6-Dinitrotoluene 20.14 165 193 N.D. (#) = qualifier out of range (m) = manual integration 28470.D GCMS1126.M Thu Nov 29 12:41:27 2001 Page 1

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NYC-WTC_000034395Source: NYC Law Department, mirrored locally

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