GCMS analysis comments for sample AD28688, Dec 2001

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Data File : C:\HPCHEM\1\DATA\DEC0401\28688.D Vial: 6 Acq On 4 Dec 2001 5:15 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 35.43 0.63 ug/l 102641 Perylene-d12 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 90) 2 Tetracosane 338 C24H50 000646-31-1 87 3 Dotriacontane 451 C32H66 000544-85-4 87 4 Octacosane 394 C28H58 nnn n-n2-a R7 undance Scan 3309 (35.426 min): 28688.D (-) m z 57.00 100.00%

5000 85

113 35154 197 225 281 35.00 35.20 35.40 35.60 35.80 m/z 71.00 66.11% rlz-> 50 100 150 200 250 300 350 400 450 bundance ' #74636: Hexatriacontane

5000 35.00 35.20 35.40 35.60 35.80 m/z 43.05 60.72% 113 141 169 197 T . 1 Jr n/z-> 50 100 150 200 250 300 350 400 450 bundance #73543: Tetracosane

35.00 35.20 35.40 35.60 35.80 5000 85 m/z 85.00 48.91%

-> thundance 50 J100 113 1555

150 183 200 250 294 300 #74490: Dotriacontane 338 350 400 450

35.00 35.20 35.40 35.60 35.80 m/z 54.95 29.65% 71 5000

97 127 155 183 379 407 450 50 100 150 200 250 300 350 400 450 35.00 35.20 35.40 35.60 35.80

28688.D GCMS1126.M Thu Dec 06 13:23:27 2001 Page 11

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