Repeat gas chromatography-mass spectrometry analysis of sample AD28596 after re-extraction, confirming bis(2-Ethylhexyl)phthalate at 0.36 ug/L with improved standard recovery of 89
NYC-WTC_000034908–000034918Folder label: “GCMS X 11/23/01 A 11/29/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC1001\28596.D Vial: 21 Acq On : 11 Dec 2001 6:14 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 15:30 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 822411 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3167927 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1575362 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 2228876 20.00 ug/1 -0.02 38) Chrysene-dl2 33.00 240 1353391 20.00 ug/1 -0.03 44) Perylene-dl2 37.10 264 907259 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 118372 4.46 ug/mL -0.02 Spiked Amount 5.000 Recovery = 89.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.43 74 4400 N.D. 3) bis(2-Chloroethyl)ether 11.11 93 8373 N.D. 4) 1,3-Dichlorobenzene 11.57 146 7993 N.D. 5) 1,4-Di chlorobenzene 11.57 146 7993 N.D. 6) 1,2-Dichlorobenzene 12.23 146 7874 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.07 117 2287 N.D. 11) Nitrobenzene 13.40 77 3869 N.D. 12) Isophorone 14.04 82 3757 N.D. 13) bis(2-Chloroethoxy)methane 14.72 93 2978 N.D. 14) 1,2,4-Trichlorobenzene 15.17 180 3162 N.D. 15) Naphthalene 15.33 128 13854 N.D. 16) Hexachlorobutadiene 15.88 225 1359 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.85 162 3451 N.D. 20) Dimethylphthalate 19.95 163 2337 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 20.09 152 3699 N.D. 2 3) Acenaphthene 20.64 153 3777 N.D. 24) 2,4-Dinitrotoluene 21.42 165 204 N.D. 25) Diethylphthalate 22.07 149 20725 N.D. 26) 4-Chlorophenyl-phenylether 22.21 204 1551 N.D. 27) Fluorene 22.18 166 3302 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 22.67 77 4148 N.D.
(#) = qualifier out of range (m) = manual integration 28596.D NP091101.M Mon Dec 17 13:10:29 2001 Page 1
NYC-WTC_000034910
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035651
Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036480
Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000034718
Document with unreadable text from DEP Box 22, folder GCMS X 11/23/01 A 11/29/01.
Filed in the same folder
NYC-WTC_000034719
Gas chromatography-mass spectrometry laboratory analytical data sheet with sample identification numbers, volumetric measurements, drip rates, and final analysis values from…
Filed in the same folder
NYC-WTC_000034722
Gas chromatography-mass spectrometry reference report listing concentrations of volatile organic compounds for sample AD28593.
Filed in the same folder
NYC-WTC_000034727
Calibration results for gas chromatography-mass spectrometry analysis showing detector responses for standard compounds.
Filed in the same folder
NYC-WTC_000034731
Instrument blank report confirming absence of target analytes in the analytical system prior to sample testing.
Filed in the same folder