Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
NYC-WTC_000036126–000036136Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C: \HPCHEM\ 1 \DATA\DEC1001\29287.D Vial: 17 Acq On : 11 Dec 2001 2:20 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 15:28 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 898717 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3442663 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1756526 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 2485300 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1538377 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1108970 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 131351 4.44 ug/mL -0.02 Spiked Amount 5.000 Recovery = 88.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 593 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.73 146 299 N.D. 5) 1,4-Dichlorobenzene 11.73 146 299 N.D. 6) 1,2-Dichlorobenzene 11.73 146 386 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 2191 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.18 165 222 N.D. 25) Diethylphthalate 22.10 149 363 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 29287.D NP091101.M Mon Dec 17 12:26:07 2001 Page 1
NYC-WTC_000036128
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NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036447
Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036029
Laboratory report noting GCMS scan results for sample AD29140 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036480
Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035820
Lab notes for sample AD29022 indicate no unusual compounds detected but one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
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