Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
NYC-WTC_000036151–000036161Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C: \HPCHEM\ 1 \DATA\DEC10 01\29231.D Vial: 24 Acq On : 11 Dec 2001 11:06 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 15:32 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 11.67 152 876606 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3374588 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1687625 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2409888 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1437845 20.00 ug/1 -0.02 44) Perylene-dl2 37.09 264 975448 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 93316 3.25 ug/mL -0.02 Spiked Amount 5.000 Recovery = 65.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.45 74 2430 N.D. 3) bis(2-Chloroethyl)ether 11.12 93 3222 N.D. 4) 1,3-Dichlorobenzene 11.58 146 1656 N.D. 5) 1,4-Dichlorobenzene 11.71 146 1957 N.D. 6) 1,2-Dichlorobenzene 12.23 146 1639 N.D. 7) 2,2’-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.06 117 588 N.D. 11) Nitrobenzene 13.24 77 402 N.D. 12) Isophorone 14.04 82 4782 N.D. 13) bis(2-Chloroethoxy)methane 14.71 93 2571 N.D. 14) 1,2,4-Trichlorobenzene 15.17 180 2074 N.D. 15) Naphthalene 15.33 128 8860 N.D. 16) Hexachiorobutadiene 15.89 225 912 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.84 162 3967 N.D. 20) Dimethylphthalate 19.95 163 5414 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 20.09 152 5566 N.D. 23) Acenaphthene 20.64 153 5282 N.D. 24) 2,4-Dinitrotoluene 21.34 165 170 N.D. 25) Diethylphthalate 22.08 149 6062 N.D. 26) 4-Chlorophenyl-phenylether 22.20 204 2171 N.D. 27) Fluorene 22.18 166 4800 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 4578 N.D. (#) = qualifier out of range (m) = manual integration 29231.D GCMS1126.M Fri Dec 14 15:33:30 2001 Page 1
NYC-WTC_000036153
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NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034908
Repeat gas chromatography-mass spectrometry analysis of sample AD28596 after re-extraction, confirming bis(2-Ethylhexyl)phthalate at 0.36 ug/L with improved standard recovery of 89
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
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NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
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NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder