Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
NYC-WTC_000036151–000036161Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\DEC1001\29231.D Vial: 24 Acq On : 11 Dec 2001 11:06 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 15:32 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenyl amine 22.62 168 1661 N.D. 31) 4-Bromophenyl-phenylether 23.67 248 999 N.D. 32) Hexachlorobenzene 24.08 284 1586 N.D. 3 3) Phenanthrene 25.18 178 5875 N.D. 34) Anthracene 25.18 178 5875 N.D. 35) Di-n-butylphthalate 26.99 149 23969 N.D. 36) Fluoranthene 28.67 202 5660 N.D. 39) Pyrene 29.34 202 6124 N.D. 40) Butylbenzylphthalate 31.49 149 1996 N.D. 41) Benzo(a)anthracene 32.95 228 10785 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 36751 0.42 ug/1 # 99 43) Chrysene 33.08 228 8713 N.D. 45) Di-n-Octylphthalate 35.04 149 4694 N.D. 46) Benzo(b)fluoranthene 36.05 252 4804 N.D. 47) Benzo(k)fluoranthene 36.11 252 5632 N.D. 4 8) Benzo(a)pyrene 36.93 252 2979 N.D. 4 9) Indeno(1,2,3 -cd)pyrene 40.82 276 1133 N.D. 50) Dibenz(a,h)anthracene 40.89 278 287 N.D. 51) Benzo(g,h,i)perylene 41.91 276 1736 N.D.
(#) = qualifier out of range (m) = manual integration 29231.D GCMS1126.M Fri Dec 14 15:33:34 2001 Page 2
NYC-WTC_000036154
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NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034908
Repeat gas chromatography-mass spectrometry analysis of sample AD28596 after re-extraction, confirming bis(2-Ethylhexyl)phthalate at 0.36 ug/L with improved standard recovery of 89
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
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Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
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NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder