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GCMS analysis report sample AD29229, Dec 2001

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Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.

NYC-WTC_000036325–000036336

Folder label: “GCMS X 12/4/01 A 12/10/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1201\29229.D Vial: 12 Acq On : 12 Dec 2001 12:44 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 19 12:48 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 910 N.D. 34) Anthracene 25.15 178 181 N.D. 35) Di-n-butylphthalate 26.99 149 48412 0.29 ug/1 98 36) Fluoranthene 28.68 202 208 N.D. 3 9) Pyrene 29.37 202 925 N.D. 40) Butylbenzylphthalate 31.49 149 1240 N.D. 41) Benzo.(a) anthracene 33.08 228 7516 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 15772 N.D. 43) Chrysene 33.08 228 7516 N.D. 45) Di-n-Octylphthalate 35.01 149 2447 N.D. 46) Benzo(b)fluoranthene 36.11 252 7181 N.D. 47) Benzo(k)fluoranthene 36.11 252 7180 N.D. 48) Benzo(a)pyrene 36.94 252 1805 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 41.93 276 397 N.D.

(#) = qualifier out of range (m) = manual integration 29229.D GCMS1126.M Fri Dec 28 15:25:24 2001 Page 2

NYC-WTC_000036328

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NYC-WTC_000036328Source: NYC Law Department, mirrored locally

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