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GCMS comments for sample AD28595, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28595 analyzed in early December 2001.

NYC-WTC_000034759–000034780

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\DEC0601\28594.D Vial: 3 Acq On 6 Dec 2001 1:05 pm Operator: 209 GALOS Sample : re extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.606 275 279 292 rBV 444176 1036842 10.90% 1.992% 2 11.343 681 686 691 rBV 156792 337849 3.55% 0.649% 3 11.416 691 694 711 rVB 158424 415376 4.37% 0.798% 4 11.673 714 722 738 rBV 2938704 7332535 77.07% 14.087% 5 15.281 1106 1115 1132 rBV 4113778 9001674 94.61% 17.294% 6 20.560 1682 1690 1707 rBV 4136123 9514355 100.00% 18.279% 7 24.975 2163 2171 2183 rBV2 3953447 9118843 95.84% 17.519% 8 25.122 2183 2187 2200 rVB 36061 111905 1.18% 0.215% 9 30.052 2718 2724 2732 rBV 492238 985581 10.36% 1.894% 10 33.017 3037 3047 3065 rBV2 3059951 7339823 77.14% 14.101% 11 33.293 3071 3077 3085 rBV 101112 220699 2.32% 0 .424% 12 35.790 3344 3349 3357 rBV 40267 105617 1.11% 0.203% 13 37.112 3484 3493 3513 rBV2 2209341 6529541 68.63% 12.545%

Sum of corrected areas: 52050640 28594.D GCMS1126.M Thu Dec 06 15:01:11 2001

NYC-WTC_000034763

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NYC-WTC_000034763Source: NYC Law Department, mirrored locally

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