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GCMS analysis comments for sample AD28147, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS scan results and recovery rates for environmental sample AD28147 analyzed in December 2001.

NYC-WTC_000033874–000033883

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\DEC0501\28147.D Vial: 7 Acq On 5 Dec 2001 6:30 pm Operator: 209 GALOS Sample re extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks; 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.644 279 283 316 rBV 246819 806322 14.55% 2.949% 2 11.711 721 726 746 rBV 1534060 4112492 74.19% 15.039% 3 15.319 1113 1119 1137 rBV 2405365 5391510 97.27% 19.716% 4 20.589 1686 1693 1709 rBV 2492592 5543037 100.00% 20.270% 5 25.004 2167 2174 2186 rBV2 2319879 4986754 89.96% 18.236% 6 30.081 2721 2727 2736 rBV 267654 549870 9.92% 2.011% 7 33.037 3042 3049 3063 rBV2 1398117 3327194 60.02% 12.167% 8 33.313 3074 3079 3087 rVB2 45790 112842 2.04% 0.413% 9 35.589 3322 3327 3338 rBV2 27471 89287 1.61% 0.327% 10 37.122 3487 3494 3512 rBV2 854053 2426657 43.78% 8.874%

Sum of corrected areas: 27345965 28147.D GCMS1126.M Thu Dec 06 08:38:23 2001

NYC-WTC_000033879

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NYC-WTC_000033879Source: NYC Law Department, mirrored locally

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