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GCMS comments for sample AD28163, Dec 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28163 dated December 6, 2001, noting no unusual compounds and low recovery rates for LCS standards.

NYC-WTC_000033847–000033855

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\l\DATA\DEC0501\28163.D Vial: 10 Acq On 5 Dec 2001 9:25 pm Operator: 209 GALOS Sample re extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.654 281 284 295 rBV 47072 137752 2.29% 0.476% 2 11.712 721 726 745 rBV 1681783 4396850 72.94% 15.193% 3 15.311 1113 1118 1135 rBV 2621143 5757038 95.50% 19.894% 4 20.589 1686 1693 1719 rBV 2685664 6028053 100.00% 20.830% 5 25.005 2167 2174 2186 rBV2 2492109 5427657 90.04% 18.755% 6 25.152 2186 2190 2198 rVB2 22404 65551 1.09% 0.227% 7 30.082 2722 2727 2737 rVB 289240 604377 10.03% 2.088% 8 33.038 3042 3049 3067 rBV2 1556294 3705439 61.47% 12.804% 9 37.132 3487 3495 3515 rBV2 962872 2816501 46.72% 9.732%

Sum of corrected areas: 28939218 28163.D GCMS1126.M Thu Dec 06 08:42:05 2001

NYC-WTC_000033852

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NYC-WTC_000033852Source: NYC Law Department, mirrored locally

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NYC-WTC_000033856

Analytical commentary for sample AD28141 dated December 6, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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