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GCMS comments for sample AD28141, Dec 2001

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Analytical commentary for sample AD28141 dated December 6, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.

NYC-WTC_000033856–000033864

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\l\DATA\DEC0501\28161.D Vial: 8 Acq On 5 Dec 2001 7:28 pm Operator: 209 GALOS Sample re extract Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.639 279 283 315 rBV 357150 1034797 16.38% 3.238% 2 11.715 721 727 743 rBV 1753204 4644641 73.53% 14.535% 3 15.314 1113 1119 1133 rBV 2859871 6099845 96.57% 19.088% 4 20.583 1687 1693 1709 rBV 2875859 6316683 100.00% 19.767% 5 25.008 2168 2175 2186 rBV2 2604660 5784008 91.57% 18.100% 6 25.155 2186 2191 2200 rVB 23821 75411 1.19% 0.236% 7 30.076 2722 2727 2734 rBV 335705 658993 10.43% 2.062% 8 33.032 3041 3049 3066 rBV2 1691627 4117497 65.18% 12.885% 9 33.316 3075 3080 3090 rBV 52832 137444 2.18% 0.430% 10 37.126 3488 3495 3524 rBV2 1100043 3086547 48.86% 9.659%

Sum of corrected areas: 31955866 28161.D GCMS1126.M Thu Dec 06 08:35:36 2001

NYC-WTC_000033861

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NYC-WTC_000033861Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28163, Dec 2001 · Box DEP Box 21

NYC-WTC_000033847

Analytical commentary for sample AD28163 dated December 6, 2001, noting no unusual compounds and low recovery rates for LCS standards.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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