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GCMS analysis results for sample AD27775, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD27775 conducted on January 2, 2002, noting unknown compounds and surrogate recovery.

NYC-WTC_000034436–000034446

Folder label: “GCMS X 11/21/01 A 12/21/01

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Scanned page image, NYC-WTC_000034442
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

'Data File : C:\HPCHEM\l\DATA\DEC1901\27775.D Vial: 24 Acq On : 21 Dec 2001 4:56 am Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.838 323 327 337 rVB 205521 409822 4.07% 0.809% 2 11.855 759 765 776 rBV 3776382 7555123 75.04% 14.914% 3 15.468 1151 1159 1176 rBV 4009145 10068656 100.00% 19.875% 4 20.750 1726 1735 1759 rBV 3935119 9827103 97.60% 19.399% 5 25.161 2205 2216 2227 rBV2 4192159 9352782 92.89% 18.462%

6 25.289 2227 2230 2239 rVB 45921 103112 1.02% 0.204% 7 33.166 3080 3089 3103 rBV2 3223286 7877589 78.24% 15.550% 8 35.679 3358 3363 3376 rBV 133816 361589 3.59% 0.714% 9 37.256 3526 3535 3547 rVB2 1788053 5103056 50.68% 10.073%

Sum of corrected areas: 50658832

27775.D NP112701.M Fri Dec 28 09:29:48 2001

NYC-WTC_000034442

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NYC-WTC_000034442Source: NYC Law Department, mirrored locally

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