GCMS analysis results for sample AD28470, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2701\28470.D Vial: 20 Acq On : 28 Nov 2001 1:48 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

11.56 0.55 ug/1 153922 1,4-Dichlorobenzene-d4 11.69

Hit# of 5 Te: tive ID MW MolForm CAS# . Qual

1 1,4-Dichlo enzene-d4 150 C6C12D4 003855-82-1 86 2 Benzene-1 , 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 27 3 Bipheny ne 152 C12H8 000259-79-0 9 4 Benzo [ thiophene-4-ol 150 C8H6OS 003610-02-4 7 Abundance Scan 709 (11.557 min): 28470.D (-) m/z 149.90 ,100.00% 150

5000 115

52 78 TI 11.20 11.40 11.60 11.80

miz-> 30 TIt.++ 50 40

40 +6160—70 80 879094 100 110 120 130 140 150 160 m/z 151.90 11 ''"'i " ■11" — — 1 — '*I ' 64.40% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 11.20 11.40 11.60 11.80 52 78 m/z 115.00 . 37.02% 35 । । I |'i ' I । । I' T ’ 1 i' ' ' ■ i ' • ........... ,,.1,1.......... — - mlz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 ‘I T T T 115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 18.77%

35 87 —.......... - ■ ■ i ■ ■ • ' l " 60 70 I i ' '' ' I ' 1 •' i ■ ' • ■ i ■ ■ 111 " " I " " I " 80 90 100 110 120 130 140 150 160 I— n/z-> 30 40 50 Abundance #67017: Biphenylene 152 11.20 11.40 11.60 11.80 m/z 52.00 . 15.63% 5000

63 76 — 97 ' I ' * 1TTT 1111 r‘‘t 11111।. .1. ।।I 126 mtz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28470.D GCMS1126.M Fri NOV 30 13:13:50 2001 Page 1

NYC-WTC_000034400