Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
NYC-WTC_000034198–000034212Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV2601\28269.D vial: 24 Acq On : 27 NOV 2001 11:10 am Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********************************************************************. Peak Number 6 dl-Xylitol, cyclic 2,3-(phenyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
43.98 2.79 ug/1 281296 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 dl-Xylitol, cyclic 2,3-(phenylboron 238 C11H15BO5 074793-46-7 22 2 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17 3 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H30O2Si4 004342-25-0 16 4 Pentanoic acid, 2-[(trimethylsilyl) 262 CllH2603Si2 055887-46-2 12 Abundance Scan 4241 (43.977 min): 28269.D (-) m/z 73.00 100.00% 73 147 221
5000 281 355 51 97 119 | 191 401 ’ 327 L . TTTTTTTTT TTTT TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT [ 253, t Im/z 146.95 U 429 43'60 43.80 44'00 44.20 44'40 98.52%
A m/z—> 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #31417: dl-Xylitol, cyclic 2,3-(phenylboronate) 147
61 _ _ 5000 104 43.60 43.80 44.00 44.20 44.40 31 177 m/z 221.0569.35%
m/z—> ___ I___ | । 207, 238__________________________ TTT——u—mur WTTu’r TCITT—ICTITOCTTTTTTTI"TTTTETTT1 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance
5000 73 #30949: Mercaptoacetic acid, bis(trimethylsilyl)- 147
221 A TTIr 43.60 43.80 44.00 44.20 44.40 m/z 281.00 34.61%
m/z—> 104 9 TVTTTTTTTTTTTTT TTTDTTUTTTT HTTTTTTTTTT 11111’711 r 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221 43.60 43.80 44.00 44.20 44.40 m/z 207.00 34.40% 73 5000 191 awaps 117 279 ......... ||, TWTVJWTUpOTp hhmlmmmmmtmpmmpmpmpmn m/z—> 20 40 60 80 100120140160180200220240260280300320340360380400420 43.60 43.80 44.00 44.20 44.40
28269.D GCMS1126.M Fri Nov 30 13:12:43 2001 Page 6
NYC-WTC_000034210
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NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder