GCMS TCLP calibration table, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\LBB.D Vial: 3 Acq On : 20 Dec 2001 5:58 pm Operator: GALOS Sample : gems unknown 11/20 Inst - : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.48 0.58 ng/uL 228648 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H120 000589-38-8 91 4 3-He: none 100 C6H120 _______ 000589-38-8 78 Abundance Scan 178 (6.475 min): LBB.D (-) m/z 43.10 100.00% 43 57

71 5000

— TT 1 1 ' i' - --A 100 39 6.20 6.40 6.60 6.80 53, 85 miz-> ml > •11 • • • • । . + ''I'"' I"'' I —TIPIPTTTTDTT ‘»i ■ > 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 "r"■r m/ z 57.10 86.92% Abundance #63358:3-Hexanone 43

5000 57

71 100 A m/z 6.20 6.40 71.05 6.60 6.80 53.28% TTTp-rrrpTnrTTTTTTT-rrTTj- IPpur ................... I I'' " r miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63357: 3-Hexanore Abundance

29 43 57 .. IA. 6.20 6.40 6.60 6.80 5000 71 m/z 100.15 28.82% 100 i, 85 11 *»* I 'I" "I"" I' ■ ■ i ■ ■ • • i ■ • ■ • i • • > • । > > > ■ । ■ ■ ■ ■ । > l11«< । ■ I"«• I" • • 11 mZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 —..........—............................. Abundance #1528: 3-Hexanone 43 57 6.20 6.40 6.60 6.80 m/z 41.10 27.42% 29 71 5000

m/z-> TTTTTTTHT TTPT ............. I' Tugp *WITTTTTT , 85 ; TTT Wpnp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100

6.20 mL 6.40 6.60 6.80

LBB.D NP112701.M Fri Dec 21 10:01:03 2001 Page 1

NYC-WTC_000034012