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GCMS unknowns analysis results for sample AD28229, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28229 conducted on January 9, 2002.

NYC-WTC_000033954–000033964

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

•Data File : C:\HPCHEM\1\DATA\NOV2601\28229.D Vial: 15 Acq On : 28 Nov 2001 6:57 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.556 705 709 719 rBV 66518 152645 1.97% 0.448% 2 11.694 719 724 741 rBV 2433342 5805696 74.86% 17.028% 3 15.302 1111 1117 1135 rBV 3614048 7636036 98.46% 22.396% 4 20.571 1685 1691 1711 rBV 3421386 7755587 100.00% 22.747% 5 24.996 2166 2173 2186 rBV2 2984954 6539632 84.32% 19.181%

6 27.007 2385 2392 2397 rBV 53866 103747 1.34% 0.304% 7 30.073 2720 2726 2733 rBV 273601 551148 7.11% 1.617% 8 33.020 3041 3047 3062 rBV2 1382153 3199811 41.26% 9.385% 9 37.114 3486 3493 3512 rBV 780456 2168102 27.96% 6.359% 10 39.593 3755 3763 3773 rBV4 18526 80854 1.04% 0.237%'

11 41.530 3965 3974 3984 rBV2 19872 101588 1.31% 0.298%

Sum of corrected areas: 34094846

28229.D GCMS1126.M Thu Jan 03 12:45:51 2002

NYC-WTC_000033959

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NYC-WTC_000033959Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28151, Nov 2001 · Box DEP Box 21

NYC-WTC_000033789

Analytical commentary for sample AD28151 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998

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