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GCMS unknowns analysis results for sample AD28326, Jan 2002

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Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28326 conducted on January 9, 2002.

NYC-WTC_000033945–000033953

Folder label: “GCMS X 11/20/01 A 11/26/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\NOV2 601\28326.D Vial: 17 Acq On : 28 Nov 2001 9:54 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 14:37 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\l\METH0DS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.70 152 1025907 20.00 ug/1 0.00 10) Naphthalene-d8 15.31 136 3862442 20.00 ug/1 0.00 17) Acenaphthene-dlO 20.57 164 1817855 20.00 ug/1 0.00 29) Phenanthrene-diO 24.99 188 2386808 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1069815 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 675480 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 105830 4.03 ug/mL 0.00 Spiked Amount 5.000 Recovery = 80.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2' -oxybis (1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.36 128 945 / N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.18 165 273/ N.D. 25) Diethylphthalate 22.08 149 1456 / N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 28326.D GCMS1126.M Mon Dec 31 14:39:09 2001 Page 1

NYC-WTC_000033947

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GCMS comments for sample AD28265, Nov 2001 · Box DEP Box 21

NYC-WTC_000033825

Analytical commentary for sample AD28265 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗
GCMS comments for sample AD28149, Nov 2001 · Box DEP Box 21

NYC-WTC_000033780

Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗

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