Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28229 conducted on January 9, 2002.
NYC-WTC_000033954–000033964Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\NOV2 601\28229.D Vial: 15 Acq On : 28 Nov 2001 6:57 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 14:40 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : NP103001
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.69 152 1110749 20.00 ug/1 0.00 10) Naphthalene-d8 15.30 136 4155139 20.00 ug/1 0.00 17) Acenaphthene-diO 20.58 164 1972602 20.00 ug/1 0.00 29) Phenanthrene-diO 25.00 188 2566138 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1020560 20.00 ug/1 -0.01 44) Perylene-dl2 37.11 264 599212 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.07 235 104972 3.72 ug/mL 0.00 Spiked Amount 5.000 Recovery = 74.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3) bis(2-Chloroethyl)ether 4) 1,3-Dichlorobenzene 5.19 0.00 0.00 74 93 146 (73)0 N.D. N.D. N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene - 0.00 146 0 N.D. 7) 2,2' -oxybis (1 -Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.00 77 (196) N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.36 128 1097 J N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.01 165 457 / N.D. 25) Diethylphthalate 22.10 149 633 / N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 28229.D GCMS1126.M Mon Dec 31 14:42:03 2001 Page 1
NYC-WTC_000033956
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NYC-WTC_000033789
Analytical commentary for sample AD28151 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033731
Laboratory report detailing GCMS analysis of sample AD28145 conducted on November 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033742
Analytical commentary for sample AD28153 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033945
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28326 conducted on January 9, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035967
Laboratory report documenting GCMS scan results for sample AD29138 with no unusual compounds detected.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017770
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30356 conducted on January 10, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019070
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30115 conducted on January 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019163
Gas chromatography-mass spectrometry analysis report for sample AD30315, completed January 9, 2002, showing unknown compounds data.
Similar document embedding; no shared entity or topic indexed. · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035820
Lab notes for sample AD29022 indicate no unusual compounds detected but one LCS compound outside acceptance range.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035990
Laboratory report noting detection of bis(2-Ethylhexyl)phthalate in sample AD29028 analyzed on December 18, 2001.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036029
Laboratory report noting GCMS scan results for sample AD29140 with one compound recovery outside acceptance range.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
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Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
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NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
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