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GCMS analysis results for sample AD30015, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD30015 conducted on January 28, 2002.

NYC-WTC_000037289–000037300

Folder label: “GCMS X 12/11/01 A 12/18/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1801\30015.D Vial: 12 Acq On : 19 Dec 2001 2:50 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 11:01 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 939247 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3606157 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1799072 20.00 ug/1 -0.02 29) Phenanthrene-dlO 24.97 188 2570512 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 24 0 1671061 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 1078376 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.06 235 138588 4.90 ug/mL -0.01 Spiked Amount 5.000 Recovery = 98.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.31 74 189 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 2 044 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.56 153 126 N.D. 24) 2,4-Dinitrotoluene 21.18 165 100 N.D. 25) Diethylphthalate 22.10 149 1249 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30015.D GCMS1126.M Tue Jan 15 11:02:19 2002 Page 1

NYC-WTC_000037291

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NYC-WTC_000037291Source: NYC Law Department, mirrored locally

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