GCMS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\28327.D Vial: 5 Acq On 8 Jan 2002 4:16 pm Operator: 209 GALOS Sample 508 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 l,4-Dichlorobenzene-d4 Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

11.39 0.52 ug/1 186325 1,4-Dichlorobenzene-d4 11.53

Hit# of )5 Tentative ID MW MolForm CAS# Qual

1 1,4-EJichlorobenzene-d4 150 C6C12D4 003855-82-1 97 2 Be: zene-l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 72 3 1, ,5-Trithiepane 152 C4H8S3 006576-93-8 7 4 penzofuran. 7-chloro- 152 C8H5C1O 024410-55-7 7 Abundance T ' Scan 691 (11.391 min): 28327.D 0 m/z 150.00 100.00% 150

5000 115 52 78 38 11.00 11.20 11.40 11.60 11.80 —445.++63— 721 —8790 99100’ 110 120’130 140150 m/z 151.90 . 63.52% m/z-> 30 40 50 60 70 80 160 Abundance #9593: 1,4-Dichlorobenzene-d4 150

5000 115 52 78 11.00 1120 1140 11.60 11.80 m/z / 35 87 TIT • '1 ' i 1 ’‘'i T-rj-t-r-nn~<-r i1 ‘ ' i TITTTT TT ।... 111।. '11' miz-2 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance 89592: Benzo =-1.2.3,4-d4-, 5,8-dichloro- 150

115 11.00 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 30.18%

35 87 Vp-T-TTT-p-rTTp T-rp-r-r-T-p-T TPTUTTTTTTTTT IPPPTPTTT miz-> 30 40 50 60 70 80 90_ 100 110 120 130 140 150 160 Abundance #10068:1,2,5-Trithiepane . ........... . 152 11.00 11.20 11.40 11.60 11.80 m/z 52.00 . 28.42% 5000 60 87 45 78 106 124

miz-> TIIBT—TTr M i1 • rp-r +196 yrr TTIT—nT[r 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.00 11.20 11.40 11.60 11.80

28327.D GCMS1126.M Wed Jan 09 09:14:43 2002 Page 1

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